resumo
Scanning thermal microscopy (SThM) is a scanning probe technique aimed at quantitative characterization of local thermal properties at the length scale down to tens of nanometers. With many probe designs and approaches to interpretation of probe responses, there is a need for a universal framework, which would allow probe calibration and comparison of probe performance. Herein, a calibration framework based on an abstracted, formal, probe model for active SThM probes is developed. The calibration can be accomplished through measurements with two or three calibration samples. Requirements for calibration samples are described with examples of structures of suitable samples identified in published literature. A link to a published experimental work indirectly verifying the proposed procedure is provided. The calibration does not require knowledge of internal probe properties and yields a small and universal set of parameters that can be used to quantify thermal resistance presented to the probe by samples as well as to characterize active-mode SThM probes of any type and at any measurement frequency. How the probe calibration parameters can be used to guide probe design is illustrated. When the calibration approach can be used directly to measure the thermal conductivity of unknown samples is also analyzed. With a large variety of operational principles and designs of probes for active-mode scanning thermal microscopy, it is highly desirable to have a unified approach to probe calibration and a broadly applicable framework that would allow comparing different probes. Here, a framework employing an analytical method routinely used in electrical engineering is developed.image (c) 2024 WILEY-VCH GmbH
palavras-chave
CONDUCTIVITY MEASUREMENTS; SPREADING RESISTANCE; SPATIAL-RESOLUTION; FLUX TUBES; MICROSCOPY; FABRICATION; CHANNELS; FILMS
categoria
Materials Science
autores
Tselev, A
nossos autores
Alexander Tselev
Investigador PrincipalProjectos
CICECO - Aveiro Institute of Materials (UIDB/50011/2020)
CICECO - Aveiro Institute of Materials (UIDP/50011/2020)
Associated Laboratory CICECO-Aveiro Institute of Materials (LA/P/0006/2020)
agradecimentos
This work was supported by the author's individual contract 2021.03599.CEECIND/CP1659/CT0016 (DOI: ) through national funds provided by FCT, Fundacao para a Ciencia e a Tecnologia, and by the project CICECO-Aveiro Institute of Materials, UIDB/50011/2020 (DOI: ), UIDP/50011/2020 (DOI: ), and LA/P/0006/2020 (DOI: ), financed by national funds through the FCT/MCTES (PIDDAC).