Synthesis and characterisation of a new vanadyl oxalatophosphate compound: (C10H10N2)[(VO)(HPO4)](2)(C2O4)
authors Shi, FN; Paz, FAA; Rocha, J; Klinowski, J; Trindade, T
nationality International
journal INORGANICA CHIMICA ACTA
author keywords vanadyl oxolatophosphate; hybrid material; crystal structure
keywords CADMIUM-ORGANIC FRAMEWORK; CRYSTAL-STRUCTURES; STRUCTURAL-CHARACTERIZATION; HYDROTHERMAL SYNTHESIS; MAGNETIC-PROPERTIES; OXALATO LIGANDS; COMPLEXES; CATIONS; MOLYBDOVANADATES; VANADIUM(V)
abstract A new vanadyl oxalatophosphate compound, (C10H10N2)[(VO)(HPO4)](2)(C2O4), was synthesized via the hydrothermal approach and characterised structurally using single-crystal X-ray diffraction, FT-IR and thermogravimetric analysis. The compound has two-dimensional {[(VO)(HPO4)](2)(C2O4)}(n)(2n-) anionic layers with C10H10N22+ occupying the interlayer spaces. (c) 2004 Elsevier B.V. All rights reserved.
publisher ELSEVIER SCIENCE SA
issn 0020-1693
year published 2005
volume 358
issue 4
beginning page 927
ending page 932
digital object identifier (doi) 10.1016/j.ica.2004.10.017
web of science category Chemistry, Inorganic & Nuclear
subject category Chemistry
unique article identifier WOS:000227507800009
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