NMR signal enhancement of more than 50 000 times in fast dissolution dynamic nuclear polarization
| authors | Luiz F. Pinto, Ildefonso Marin-Montesinos, Vega Lloveras, José Luís. Muñoz-Gómez, Miquel Pons, Jaume Veciana, José Vidal-Gancedo |
| nationality | International |
| journal | Chemical Communications |
| abstract | Herein, we report the synthesis and the study of a novel mixed biradical with BDPA and TEMPO radical units that are covalently bound by an ester group (BDPAesterTEMPO) as a polarizing agent for fast dissolution DNP. The biradical exhibits an extremely high DNP NMR enhancement of >50 000 times, which constitutes one of the largest signal enhancements observed so far, to the best of our knowledge. |
| year published | 2017 |
| volume | 53 |
| beginning page | 3757 |
| digital object identifier (doi) | 10.1039/C7CC00635G |
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| journal impact factor | 5.996 |
| 5 year journal impact factor | 5.818 |
| category normalized journal impact factor percentile | 81.073 |
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