A general soft-chemistry route to metal phosphate nanocrystals

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abstract

The "benzyl alcohol route" was extended for the synthesis of various metal phosphate nanocrystals. The proposed one pot reaction leads to narrocrystalline titanium, zirconium, vanadium, yttrium and lanthanide phosphates at a yield above 90%. The synthesized particles are characterized by a high crystallinity and a small size distribution. (C) 2009 The Korean Society of Industrial and Engineering Chemistry. Published by Elsevier B.V. All rights reserved.

keywords

SOL-GEL SYNTHESIS; LIQUID-PHASE SYNTHESIS; OXIDE NANOPARTICLES; NONAQUEOUS SYNTHESIS; VANADIUM PHOSPHATE; LAPO4-RE RE; CE; LUMINESCENCE; PHOSPHONATES; PARTICLES

subject category

Chemistry; Engineering

authors

Willinger, MG; Clavel, G; Di, WH; Pinna, N

our authors

foto Nicola Pinna

Nicola Pinna

Researcher

Groups

Projects

RMNE-UA-National Network of Electron Microscopy (REDE/1509/RME/2005 )

Functionalised Advanced Materials and Engineering of Hybrids and Ceramics - FAME (FAME)

acknowledgements

Sonia S. Nobre and Rute A. S. Ferreira from CICECO, University of Aveiro, are acknowledged for help with emission spectroscopy and quantum yield measurements. W. Di is grateful for the supports of FCT (grant No. SFRH/BPD/4088112007). Financial support from FAME network of excellence and WCU (World Class University) program through the Korea Science and Engineering Foundation funded by the Ministry of Education, Science and Technology (4002008-0230) is acknowledged. The authors acknowledge the RNME, FCT Project: REDE/1509/RME/2005.

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Publication Details

type
Journal Article
year
2009
journal
JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY
volume
15
publisher
KOREAN SOC INDUSTRIAL ENGINEERING CHEMISTRY
issn
1226-086X
issue
6
digital object identifier
10.1016/j.jiec.2009.09.017
web of science article identifier
WOS:000273459100022

Journal Metrics (JCR 2019)

Journal Impact Factor
5.278
Journal Impact Factor (5 yrs)
5.3
category normalized journal percentile
81.674

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